By Jones W.B. (ed.), Thorn W.J. (ed.), Waadeland H. (ed.)

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Extra resources for Analytic Theory of Continued Fractions, Leon, Norway 1981: Proceedings

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For microtoming of the sample for IR microanalysis, the best results are obtained by allowing the embedment to set 3 6-4 8 hours before slicing. The medium continues to cure slowly over time ( Demmler 1 9 8 0 ) . After one month, the microtoming becomes noticeably more difficult, and the samples tend to crumble . The bottom and top halves of the block should be prepared within a few days of each other to prevent a hardness differential between halves that interferes with microtoming. Silicone molds, ice cube trays, and peel-away molds are all useful for preparing embedments; some examples are shown in Figure 3 .

At this point, photomicrographs, in visible and UV light, are taken of the cut surface, preferably adj acent to the thin section layer removed for IR analysis. Later, if desired, the embedded residual sample can be used for IR reflectance mapping studies, SEM, and fluorescent staining. The compiled data set from these analyses should give a clear image of the structural composition of the paint sample . The unembedded portion of the sample is retained for later chromatographic studies or for additional embed­ ments, if problems arise from the first sample.

Lm thick. However, depending on the absorption of the sample, this may be too thick for IR analysis. Lm thick. 1 2 thinner than 1 /-Lm. A general dictum is that harder samples require A motorized rotary microtome with a harder knives. Of the four blades, glass knives are the easiest to use. Glass stereobinocular m icroscope for viewing and positioning the sample. 54 em ( 1 inch) square of Figure 3 . 1 3 glass to create two triangular pieces, each with a very sharp edge ( Figs. A selection o f m icrotoming blades: dia­ 3 .

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Analytic Theory of Continued Fractions, Leon, Norway 1981: Proceedings by Jones W.B. (ed.), Thorn W.J. (ed.), Waadeland H. (ed.)


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Analytic Theory of Continued Fractions, Leon, Norway 1981: by Jones W.B. (ed.), Thorn W.J. (ed.), Waadeland H. (ed.) PDF
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