By Anil K. Mukherji, R. Belcher and M. Frieser (Auth.)

ISBN-10: 0080068863

ISBN-13: 9780080068862

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131, 416 (1950). SCHUMB, W. C. and NOLAN, E. , Anal. Chem. 9, 371 (1937). , Z. Anal. Chem. 117, 252 (1939). SMITH, M. M. and JAMES, C , / . Amer. Chem. Soc. 42, 1764 (1920). SIMPSON, S. C , Anal. Chem. 5, 40 (1933); 7, 36 (1935). SIMPSON, S. G. and SCHUMB, W. C , / . Amer. Chem. Soc. 53, 921 (1931). SCHUMB, W. C. and PITTMAN, F . , Anal. Chem. 14, 512 (1942). FRESENIUS, W. , Handbuch der Analytischen Chemie, Springer, Berlin, 1950, Part III, Vol. IVb. p p . 170-287. CLASSEN, A. , Rec. Trav. Chim.

Successive Determination of Zirconium and Titanium(29) After the determination of zirconium, titanium was determined in the same solution by the addition of hydrogen peroxide and excess EDTA and back-titration with bismuth nitrate. 6 N) solution as described. Cool below 20°C. Add enough EDTA to complex all the titanium. Add 5 ml of 10 % H 2 0 2 . Neutralize with aqueous ammonia (1:1) to the red-violet colour of xylenol orange. Acidify with nitric acid to pH 1-2. 05 M bismuth nitrate to an intense red color.

Appl. 19, 89 (1937). OSTROUMOV, E. , Zavod. Lab. 6, 16 (1937). WELCHER, F . , Organic Analytical Reagents, Van Nostrand, New York, 1947, Vol. 1, p. 323. 28. ALLEN, E. , / . Amer. Chem. Soc. 25, 421 (1903). 29. , Z . Anal. Chem. 78, 133 (1929); 86, 13 (1931). 30. RAY, P. and CHATTOPADHYA, A. , Z . Anorg. Chem. 169, 199 (1926). 31. HOLNESS, H . and KEAR, R. , Analyst, 74, 597 (1949). 32. PURUSHOTTAM, A. and RAGHAVA R A O , B. S. , Analyst, 75, 555 (1950). 33. PURUSHOTTAM, A. and RAGHAVA RAO, B. S.

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Analytical Chemistry of Zirconium and Hafnium by Anil K. Mukherji, R. Belcher and M. Frieser (Auth.)


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